The aim of the CD laboratory is to intensify and further deepen research in the field of Inclusion Metallurgy especially focusing on open questions from a scientific point of view as well as application-oriented subjects in cooperation with the industry partners. The principal idea is to establish a bridge from inclusion formation over their modification and evolution in the system steel-slag-refractory to their final impact on material properties for specific applications. With this approach, the primary aim is to study the relation and interaction between micro-, meso- and macro-cleanness in steel with a special focus on meso-cleanness.

Different process routes and completely various products will be investigated regarding steel cleanness related issues: From integrated steel mill with classical secondary metallurgical processes to powder metallurgical production with Electroslag Heating followed by atomization; from steels for automotive applications to cold work tool steels for precision blanking. However, basic mechanisms and scientific questions related to Inclusions Metallurgy are comparable.

Especially the further development of inclusion analytics, also considering machine learning tools to support inclusion characterization and the representative analysis of meso-particles, as well as different aspects regarding interfacial properties influencing the inclusion behavior, are in the focus of interest. Special attention will be paid on the role of different alkali and rare earth elements changing the inclusions behavior in the system steel-slag-refractory to their final impact on material properties for specific applications.

Objectives:

1. Specific creation of defined inclusion populations on laboratory scale especially considering the role of alkali and rare earth elements; Investigation of the inclusion behavior in the system steel-slag-refractory by means of different experimental methods.

2. Development of a deepened understanding regarding inclusion morphology through the combination of various methods for inclusion analytics focusing on multiphase particles.

3. Linking different analytical tools considering data-driven modeling by means of machine learning for a more efficient inclusion characterization.

4. Systematic, multi-scale analysis and tracking of non-metallic inclusions, especially for the meso-size range.

5. Establishment of isotope analysis for inclusion tracking in the system steel-slag-refractory.

With the CD laboratory, three projects are conducted in cooperation with one industry partner each:

Research Project I: NMI-PM

This project focuses on the behavior of non-metallic inclusions in the powder metallurgical production of tool and high speed steels and the therewith connected potential for further optimization of the already very high steel cleanness level. Based on a deepened understanding of the relation between specific aspects of steel cleanness and the fatigue behavior under defined stresses and loads, the need for excessive material testing should be reduced.

Industrial Partner: voestalpine Böhler Edelstahl GmbH & Co KG

Research Project II: SECMET-SURACT

The main focus of this project is on the challenges for secondary metallurgy in context with alternative routes for crude steel production based on the route Direct Reduction/Electric Arc Furnace. Especially considering the role of treatments with several (tracer) elements (e.g. alkali or lanthanide group to improve inclusion removal) will be investigated.

Industrial Partner: voestalpine Stahl Donawitz GmbH

Research Project III: MESO-INC

The aim of this project is to study the behavior of inclusions in different steel grades for automotive applications, especially considering the role and impact of meso-inclusions. For this purpose, a multi-scale inclusion characterization, as well as a systematic tracing of particles over the production process by different methods, are of significant interest and importance.

Industrial Partner: voestalpine Stahl GmbH

Scientific Cooperation: Chair of General and Analytical Chemistry, Montanuniversitaet Leoben

Head of the CD-Lab

S.K. Michelic and C. Bernhard, Significance of Nonmetallic Inclusions for the Clogging Phenomenon in Continuous Casting of Steel––A Review. steel research int. (2022), doi:10.1002/srin.202200086

W. Mu, S.K. Michelic and Q. Wang, Editorial: Inclusion/Precipitate Engineering and Thermo-Physical Properties in Liquid Steels and Alloys. Front. Mater. 9 (2022). doi:10.3389/fmats.2022.922203

Post-Doc

S. Ramesh Babu, N. Preisser and S.K. Michelic, Image Processing Procedure to Evaluate Inclusion Dissolution in a Slag Observed by High-Temperature Confocal Scanning Laser Microscopy. Metals 12 (2022), 4. doi:10.3390/met12040531

S. Ramesh Babu and S.K. Michelic, Analysis of Non-Metallic Inclusions by Means of Chemical and Electrolytical Extraction—A Review. Materials 15 (2022), 9. doi:10.3390/ma15093367

S. Ramesh Babu, R. Musi, K. Thiele and S.K. Michelic, Classification of non-metallic inclusions in steel by data-driven machine learning methods. steel research int. (2022), doi:10.1002/srin.202200617

PhD candidate

K. Thiele, R. Musi, S. Ramesh Babu and S.K. Michelic, Optimization of the Two‐ and Three‐Dimensional Characterization of Rare Earth‐Traced Deoxidation Products. Adv Eng Mater (2023), pp. 2201748. doi:10.1002/adem.202201748

K. Thiele, P. Presoly, D. Ernst, S. Ramesh Babu and S. K. Michelic, Evaluation of different alloying concepts to trace non-metallic inclusions by adding rare earths on a laboratory scale. Ironmaking & Steelmaking (2022), doi:10.1080/03019233.2022.2124816

Conferences:

K. Thiele, S. Wagner, C. Walkner, T.C. Meisel, J. Irrgeher, T. Prohaska and S.K. Michelic, Tracing the origin of non-metallic inclusions by elemental and isotopic fingerprints, Junganalytiker*innen Forum, Montanuniversitaet Leoben, Austria

K. Thiele, S. Ilie, R. Roessler, C. Walkner, T.C. Meisel, T. Prohaska and S.K. Michelic, Different Approaches to Trace the Source of Non-Metallic Inclusions in Steel. AISTech 2023, Huntington Place, Detroit, Michigan, USA

K. Thiele, S. Ilie, R. Roessler, C. Walkner, T.C. Meisel, T. Prohaska and S.K. Michelic, Different Approaches to Trace the Source of Non-Metallic Inclusions in Steel. 8th International Congress on the Science and Technology of Steelmaking (ICS), Montreal, Kanada (2022)

K. Thiele, S. Ilie, R. Rössler and S.K. Michelic, Characterization of Rare-Earth-Elements-Traced Non-Metallic Inclusions by Different Methods, 8th International Congress on the Science and Technology of Steelmaking (ICS), Montreal, Kanada (2022)

K. Thiele, C. Walkner, T.C. Meisel, T. Prohaska and S.K. Michelic, Application of ICP-MS to study the evolution of non-metallic inclusions in steelmaking, 28. ICP-MS ANWENDER*INNEN TREFFEN, Montanuniversität Leoben, Österreich (2022)

K. Thiele, S. Ilie, R. Roessler, A. Penz and S.K. Michelic, Tracing of Non-metallic Inclusions in Secondary Metallurgy by Means of Rare Earth Elements. ASIA STEEL 2021 jointed with Automotive Steel International Conference, Gyeongju, Korea (2021)

PhD candidate

J. Cejka and S. K. Michelic, In-Situ Observation of Steel/Slag/Inclusion Interaction by Means of High-Temperature Confocal Scanning Laser Microscopy. Metals (2023), doi:10.3390/met13040686

Conferences:

J. Cejka, G. Klösch, P. Presoly and S.K. Michelic. Influence of specific trace elements on the wetting behaviour of a medium-carbon steel in contact with different oxidic substrates, Material Sciene and Enginnering MSE Darmstadt, Germany (2022)